MARPOL ANNEX VI - GUIDE LINE FOR FUEL SAMPLE

RESOLUTION MEPC.96(47)
Adopted on 8 March 2002
GUIDELINES FOR THE SAMPLING OF FUEL OIL FOR DETERMINATION OF COMPLIANCE WITH ANNEX VI OF MARPOL 73/78
These guidelines were revoked by res. MEPC.182(59) of 2009-07-17
RECALLING Article 38(a) of the Convention on the International Maritime Organization concerning the functions of the Marine Environment Protection Committee (the
Committee) conferred upon it by international conventions for the prevention and control of marine pollution,
RECALLING ALSO that the Conference of Parties to the International Convention for the Prevention of Pollution from Ships, 1973, as modified by the Protocol of 1978 relating thereto (MARPOL 73/78), held in September 1997, adopted the Protocol of 1997 to amend MARPOL 73/78 with a new Annex VI on the Prevention of Air Pollution from Ships,
NOTING that regulation 18(6) on fuel oil quality within Annex VI of MARPOL 73/78 requires that the bunker delivery note shall be accompanied by a representative sample of
the fuel oil delivered taking into account guidelines to be developed by the Organization,
BEING AWARE that this requirement cannot be enforced before the entry into force of the Protocol of 1997,
BEING AWARE ALSO that relevant Guidelines have to be developed before the entry into force of the Protocol of 1997 in preparation for the implementation of Annex VI of
MARPOL 73/78,
HAVING CONSIDERED the draft Guidelines prepared by the Sub-Committee on Ship Design and Equipment at its forty-fourth session,
1 ADOPTS the Guidelines for the sampling of fuel oil for determination of compliance with Annex VI of MARPOL 73/78, as set out in the Annex to this resolution;
2 INVITES Governments to apply the Guidelines from the date of entry into force of the Protocol of 1997.
ANNEX
GUIDELINES FOR THE SAMPLING OF FUEL OIL FOR DETERMINATION OF COMPLIANCE WITH ANNEX VI OF MARPOL 73/78
TABLE OF CONTENTS
1 Preface
2 Introduction
3 Definitions
4 Sampling methods
5 Sampling and sample integrity
6 Sampling location
7 Retained Sample handling
8 Sealing of the Retained Sample
9 Retained Sample storage
1 Preface
The primary objective of these Guidelines is to establish an agreed method to obtain a representative sample of the fuel oil for combustion purposes delivered for use on board
ships.
2 Introduction
The basis for these Guidelines is regulation 18(3) of Annex VI to MARPOL 73/78, which provides that for each ship subject to regulations 5 and 6 of that Annex, details of fuel oil
for combustion purposes delivered to, and used on board the ship, shall be recorded by means of a bunker delivery note which shall contain at least the information specified in
appendix V to that Annex. In accordance with regulation 18(6) of Annex VI, the bunker delivery note shall be accompanied by a representative sample of the fuel oil delivered.
This sample is to be used solely for determination of compliance with Annex VI of MARPOL 73/78.
3 Definitions
For the purpose of these Guidelines:
3.1 Supplier's representative is the individual from the bunker tanker who is responsible for the delivery and documentation or, in the case of deliveries direct from the shore to
the ship, the person who is responsible for the delivery and documentation.
3.2 Ship's representative is the ship's master or officer in charge who is responsible for receiving bunkers and documentation.
3.3 Representative sample is a product specimen having its physical and chemical characteristics identical to the average characteristics of the total volume being sampled.
3.4 Primary sample is the representative sample of the fuel delivered to the ship collected throughout the bunkering period obtained by the sampling equipment positioned at
the bunker manifold of the receiving ship. 3.5 Retained sample is the representative sample in accordance with regulation 18(6) of Annex VI to MARPOL 73/78, of the fuel
delivered to the ship derived from the primary sample.
4 Sampling methods
The primary sample should be obtained by one of the following methods:
.1 manual valve-setting continuous-drip sampler; or
.2 time-proportional automatic sampler; or
.3 flow-proportional automatic sampler.
4.2 Sampling equipment should be used in accordance with manufacturer's instructions, or guidelines, as appropriate.
5 Sampling and sample integrity
5.1 A means should be provided to seal the sampling equipment throughout the period of supply.
5.2 Attention should be given to:
.1 the form of set up of the sampler;
.2 the form of the primary sample container;
.3 the cleanliness and dryness of the sampler and the primary sample container prior to use;
.4 the setting of the means used to control the flow to the primary sample container; and
.5 the method to be used to secure the sample from tampering or contamination during the bunker operation.
.5 the method to be used to secure the sample from tampering or contamination during the bunker operation.
5.3 The primary sample receiving container should be attached
to the sampling equipment and sealed so as to prevent tampering or contamination of the sample throughout the bunker delivery period.
6 Sampling location
For the purpose of these Guidelines a sample of the fuel delivered to the ship should be obtained at the receiving ship's inlet bunker manifold and should be drawn continuously throughout the bunker delivery period.*
________
* The phrase ' be drawn continuously throughout the bunker delivery period' in paragraph 6 of the Guidelines should be taken to mean continuous collection of drip sample
throughout the delivery of bunker fuel covering each bunker delivery note. In case of receiving an amount of bunker fuel necessitating two or more delivery notes, the sampling
work may be temporarily stopped to change sample bags and bottles and then resumed as necessary.
7 Retained sample handling
7.1 The retained sample container should be clean and dry.
7.2 Immediately prior to filling the retained sample container, the primary sample quantity should be thoroughly agitated to ensure that it is homogenous.
7.3 The retained sample should be of sufficient quantity to perform the tests required but should not be less than 400 ml. The container should be filled to 90% + or - 5%  capacity and sealed.
8 Sealing of the retained sample
8.1 Immediately following collection of the retained sample, a tamper proof security seal with a unique means of identification should be installed by the supplier's representative
in the presence of the ship's representative. A label containing the following information should be secured to the retained sample container:
.1 location at which, and the method by which, the sample was drawn;
.2 date of commencement of delivery;
.3 name of bunker tanker/bunker installation;
.4 name and IMO number of the receiving ship;
.5 signatures and names of the supplier's representative and the ship's representative;
.6 details of seal identification; and
.7 bunker grade.
8.2 To facilitate cross-reference details of the seal, identification may also be recorded on the bunker delivery note.
9 Retained sample storage
9.1 The retained sample should be kept in a safe storage location, outside the ship's accommodation, where personnel would not be exposed to vapours which may be released from the sample. Care should be exercised when entering a sample storage location.
9.2 The retained sample should be stored in a sheltered location where it will not be subject to elevated temperatures, preferably at a cool/ambient temperature, and where it will not be exposed to direct sunlight.
9.3 Pursuant to regulation 18(6) of Annex VI of MARPOL 73/78, the retained sample should be retained under the ship's control until the fuel oil is substantially consumed, but in any case for a period of not less than 12 months from the time of delivery.
9.4 The ship's master should develop and maintain a system to keep track of the retained samples.

These guidelines were revoked by res. MEPC.182(59) of 2009-07-17.
Document Links
Regulation (18) Annex VI doc. no. MARPA618ABA
Document id: RESL9647ARS
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